Synthesis and Structural Analysis of Tetrathioureacopper(I) Chloride

S. LAKSHMI; M. A. SRIDHAR; J. Shashidhara PRASAD; V. S RINIVASAN; M. A. KANDHASWAMY; M. DHANDAPANI

doi:10.2116/analscix.19.x19

October - December (2003)

Synthesis and Structural Analysis of Tetrathioureacopper(I) Chloride

S. LAKSHMI, M. A. SRIDHAR, J. Shashidhara PRASAD, V. S RINIVASAN, M. A. KANDHASWAMY, M. DHANDAPANI

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JOURNAL FREE ACCESS

2003 Volume 19 Pages x19-x20

DOI https://doi.org/10.2116/analscix.19.x19

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Abstract

Tetrathioureacoper(I) chloride was synthesised to study its NLO property. Crystals suitable for single crystal x-ray diffraction studies were grown by evaporation method. The compound crystallizes in the tetragonal system and has been characterized thus: P4₁2₁2, a = 13.4090(5) Å, c = 13.8100(4)Å, V = 2483.1(1)Å³, Z = 8, D_c = 1.751 Mg/m³. The compound does not exhibit the NOL property.

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