Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
July - September
Crystal Structure of Imide-Amide between Kemp’s Acid and L-Prolinol
Yuka ODOTetsuro SHIMOMasaru KAWAMINAMIKenichi SOMEKAWA
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2004 Volume 20 Pages x119-x120

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Abstract

The title compound was synthesized from the reaction of Kemp’s imide acid with L-prolinol. It crystallized in tetragonal space group P41212 with cell parameters a = 11.893(2)Å, c = 23.730(3)Å and Z = 8. The structure exhibits an intramolecular hydrogen bond of the type C=O…HO between one imide carbonyl group and a hydroxyl group in the L-prolinol moiety, and also an intermolecular hydrogen bond of the type NH…O.

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© 2004 by The Japan Society for Analytical Chemistry
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