Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 12
Crystal Structure of N-(α-(1-Phenyl-3-methyl-5-pyrazolone-4-ylidene)benzyl)-N′-3,4,5-trimethoxybenzoylhydrazine
Yifeng SUNDongdi ZHANGHongyin GAOHuicheng WANGRuojie TAO
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JOURNAL FREE ACCESS

2006 Volume 22 Pages x289-x290

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Abstract
The title compound, C27H26N4O5, was synthesized by the condensation of 1-phenyl-3-methyl-4-benzoylpyrazolone-5 and 3,4,5-trimethoxybenzoylhydrazide. The crystal structure was determined by single-crystal X-ray diffraction. It crystallizes in the triclinic system, space group P1 with a = 9.1895(18)Å, b = 12.201(2)Å, c = 12.500(3)Å, α = 78.32(3)°, β = 74.23(3)°, γ = 68.86(3)°, V = 1249.4(4)Å3, Z = 2, R = 0.0605. The inter- or intramolecular N-H…O hydrogen bonds, together with π-π stacking interactions, stabilize the crystal structure by causing the formation of a one-dimensional chain structure.
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© 2006 by The Japan Society for Analytical Chemistry
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