BUNSEKI KAGAKU
Print ISSN : 0525-1931
Technical Papers
SEM-EDX Analysis of Insulator Specimen by Using Garment Antistatic Spray
Long ZESusumu IMASHUKUJun KAWAI
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2013 Volume 62 Issue 2 Pages 155-158

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Abstract

SEM-EDX analyses of insulator samples are usually believed to be difficult because of charge-up effect, and thus carbon or gold evaporation was performed prior to the SEM observation. However, such an electric conductive thin film will emit characteristic X-rays, interfering the EDX analysis. In the present study, we report that using an anti-static spray is an easier and more effective way than using an ionic liquid. Possibility of metal corrosion by the anti-static spray should be noted.

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© The Japan Society for Analytical Chemistry 2013
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