BUNSEKI KAGAKU
Print ISSN : 0525-1931
Rapid determination of aluminum, chlorine, titanium and iron in polyethylene by X-ray fluorescence spectrometry
Seiju HAYASHIKoji SUGAHARAKiyoshi TERANISHI
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1967 Volume 16 Issue 12 Pages 1328-1335

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Abstract
A fluorescent X-ray method was proposed for the rapid determination of aluminum, chlorine, titanium and iron in high-density polyethylene.
The calibration curves were drawn on synthetic standards prepared by mixing standard materials (aluminum oxide, sodium chloride, titanium oxide and ferric oxide) each corresponding to 5400 ppm of the inspected element into purified high-density polyethylene.
The method is five to seven times more rapid than chemical procedures, and the accuracies were, Al: σ = 112% for 50400 ppm, Cl: σ =42% for 50400 ppm, Ti: σ =182% for 3100 ppm, and Fe: σ=242% for 1100 ppm.
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© The Japan Society for Analytical Chemistry
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