GEOCHEMICAL JOURNAL
Online ISSN : 1880-5973
Print ISSN : 0016-7002
ISSN-L : 0016-7002
Note
Determination of 9Be in geological standard samples, JA-2 and JB-2, and of 9Be and 10Be in a basaltic rock sample for evaluation of uncertainty involved in 10Be/9Be ratio measurements
KATSUNORI GOTANSHUN'ICHI NAKAIHIROYUKI MATSUZAKI
Author information
Keywords: 10Be, 9Be, ICP-MS, AMS, uncertainty
JOURNAL FREE ACCESS

2008 Volume 42 Issue 3 Pages 305-308

Details
Abstract
We determined the concentrations of 9Be in JB-2 and JA-2 geological standard samples using an inductively coupled plasma mass spectrometer (ICP-MS). We determined 9Be abundance in standard samples of JA-2 and JB-2 as 2.26 ± 0.10 and 0.241 ± 0.010 ppm, respectively, after comparing and selecting 9Be concentration data obtained by the internal standard method, the standard addition method and the column separation method. In the course of comparison, we identified a problem in the internal standard method, which is usually used for abundance analyses using an ICP-MS. Repeated analyses of a basalt lava gave a standard deviation of 10Be abundance of 9% (1σ, n = 5). From the results, we estimated the uncertainty of 10Be/9Be ratio as 10% (1σ), considering a law of propagation of errors.
Content from these authors
© 2008 by The Geochemical Society of Japan
Previous article
feedback
Top