Solid-state synthesis of zirconium nitride and hafnium nitride powders

Ze-Ying WU; Zhe CHEN; Liangbiao WANG; Liwei FANG; Tingting ZHOU; Tao MEI; Ciyang ZHANG; Qianwen LI

doi:10.2109/jcersj2.20177

Notes

Solid-state synthesis of zirconium nitride and hafnium nitride powders

Ze-Ying WU, Zhe CHEN, Liangbiao WANG, Liwei FANG, Tingting ZHOU, Tao MEI, Ciyang ZHANG, Qianwen LI

Author information

Ze-Ying WU
School of Chemical Engineering and Materials, Changzhou Institute of Technology
Zhe CHEN
School of Chemistry and Environment Engineering, Jiangsu University of Technology
Liangbiao WANG
School of Chemistry and Environment Engineering, Jiangsu University of Technology
Liwei FANG
School of Chemistry and Environment Engineering, Jiangsu University of Technology
Tingting ZHOU
School of Chemistry and Environment Engineering, Jiangsu University of Technology
Tao MEI
Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Ministry of Education, Key Laboratory for the Green Preparation and Application of Functional Materials, School of Materials Science and Engineering, Hubei University
Ciyang ZHANG
School of Chemistry and Environment Engineering, Jiangsu University of Technology
Qianwen LI
College of Light-Textile Engineering and Art, Anhui Agriculture University

Keywords: Nitride, Chemical synthesis, Powders, X-ray diffraction

JOURNAL OPEN ACCESS

2021 Volume 129 Issue 3 Pages 200-203

DOI https://doi.org/10.2109/jcersj2.20177

Details

Abstract

Zirconium nitride (ZrN) powders have been prepared by using the zirconium dioxide (ZrO₂), sodium azide (NaN₃) and metallic magnesium (Mg) as starting materials in a stainless-steel autoclave. The X-ray powder diffraction pattern indicates the formation of cubic phase ZrN. Hafnium nitride (HfN) can also be synthesized from hafnium dioxide (HfO₂) through the similar procedure.

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