Journal of the Ceramic Society of Japan
Online ISSN : 1348-6535
Print ISSN : 1882-0743
ISSN-L : 1348-6535
Technical reports
In-house-built single-crystal anomalous X-ray diffraction measurement system using white X-rays and an energy dispersive detector
Rayko SIMURAHisanori YAMANETerutoshi SAKAKURAKazumasa SUGIYAMA
Author information
JOURNALS FREE ACCESS

2021 Volume 129 Issue 9 Pages 594-600

Details
Abstract

A single crystal X-ray diffraction (XRD) measurement system composed of white X-rays from an in-house X-ray generator, a four-circle diffractometer, and a compact energy dispersive detector was constructed to acquire XRD data including the effect of anomalous scattering of X-rays with selective energy. The obtained data are available for crystal structure analysis to determine the atomic positions of a specific element by the δ-synthesis method. A single crystal of Sr3Y(BO3)3 containing neighboring elements of Sr and Y, which could not be distinguished by conventional XRD analysis, was tested to demonstrate the performance of the present system.

Information related to the author
© 2021 The Ceramic Society of Japan

この記事はクリエイティブ・コモンズ [表示 - 改変禁止 4.0 国際]ライセンスの下に提供されています。
https://creativecommons.org/licenses/by-nd/4.0/deed.ja
Previous article Next article
feedback
Top