Journal of the Ceramic Society of Japan
Online ISSN : 1348-6535
Print ISSN : 1882-0743
ISSN-L : 1348-6535
Technical reports
In-house-built single-crystal anomalous X-ray diffraction measurement system using white X-rays and an energy dispersive detector
Rayko SIMURAHisanori YAMANETerutoshi SAKAKURAKazumasa SUGIYAMA
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2021 Volume 129 Issue 9 Pages 594-600

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Abstract

A single crystal X-ray diffraction (XRD) measurement system composed of white X-rays from an in-house X-ray generator, a four-circle diffractometer, and a compact energy dispersive detector was constructed to acquire XRD data including the effect of anomalous scattering of X-rays with selective energy. The obtained data are available for crystal structure analysis to determine the atomic positions of a specific element by the δ-synthesis method. A single crystal of Sr3Y(BO3)3 containing neighboring elements of Sr and Y, which could not be distinguished by conventional XRD analysis, was tested to demonstrate the performance of the present system.

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© 2021 The Ceramic Society of Japan

この記事はクリエイティブ・コモンズ [表示 - 改変禁止 4.0 国際]ライセンスの下に提供されています。
https://creativecommons.org/licenses/by-nd/4.0/deed.ja
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