Chemical synthesis of rod-like cobalt phosphide

Qingting Ni; Zixun Huang; Liangbiao Wang; Jie Sui; Da Huang; Taotao Yun; Jiali Dai; Tinghai Yang; Xiaokai Song

doi:10.2109/jcersj2.23147

Full papers

Chemical synthesis of rod-like cobalt phosphide

Qingting Ni, Zixun Huang, Liangbiao Wang, Jie Sui, Da Huang, Taotao Yun, Jiali Dai, Tinghai Yang, Xiaokai Song

Author information

Qingting Ni
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology
Zixun Huang
School of Resources and Environmental Engineering, Jiangsu University of Technology
Liangbiao Wang
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology
Jie Sui
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology
Da Huang
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology
Taotao Yun
Jiangsu Changli Testing Service Co., Ltd.
Jiali Dai
Jiangsu Guorun Testing Service Co., Ltd.
Tinghai Yang
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology
Xiaokai Song
School of Chemistry and Chemical Engineering, School of Chemistry & Chemical Engineering, Jiangsu Laboratory of Precious Metals Processing Technology and Application, Jiangsu University of Technology

Keywords: Chemical synthesis, Rod-like, Cobalt phosphide, X-ray diffraction

JOURNAL OPEN ACCESS

2024 Volume 132 Issue 1 Pages 8-10

DOI https://doi.org/10.2109/jcersj2.23147

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Abstract

In this paper, we have successfully prepared orthorhombic phase cobalt phosphide by a facile one-step method. The synthesis reaction is carried out in an autoclave using cobaltic oxide as a Co-source and red phosphorous as P-source. The phase and the morphology of the samples were characterized by X-ray diffraction (XRD), scanning electron microscopes (SEM), transmission electron microscopes (TEM) and high resolution transmission electron microscope (HRTEM).

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