Introduction and Practice of Crystal Structure Refinement Using SHELXL-2014
Let's Use SHELXL against Merohedral Twinning !
2015 Volume 57 Issue 5 Pages 269-275
Details
2015 Volume 57 Issue 5 Pages 269-275
In this tutorial course of SHELXL, we will focus on how to treat the twinning by merohedry. Merohedral twinning is not apparent during the measurement or in the diffraction pattern, and therefore, unsolved twinning and fuzzy molecular structures remain in the data folder. We would like to show the avoidable pitfalls that are to be considered for the correct molecular structures using examples of solved merohedral twin crystals and step by step tutorials for organ(ometall)ic chemists.
