Nihon Kessho Gakkaishi
Online ISSN : 1884-5576
Print ISSN : 0369-4585
ISSN-L : 0369-4585
Direct Observation of a Temperature (Debye-Waller) Factor Anomaly at Specific Atomic Sites by Annular-Dark-Field STEM
Eiji ABE
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2003 Volume 45 Issue 6 Pages 378-383

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Abstract
A real-space imaging of a local thermal vibration anomaly in a solid has been demonstrated for the first time, through atomic-resolution annular dark-field scanning transmission electron microscope (ADF-STEM) observations of an Al72Ni20Co8 quasicrystalline compound. Significant changes of ADF-contrast depending on the observation temperature as well as the scattering angle ranges are found to be obvious at some particular Al atomic sites. The origin of this anomalous ADF-contrast is explained fairly well by the thermal diffuse scattering (TDS) intensity change due to different values of temperature (Debye-Waller) factor, which is defined by mean-square thermal vibration amplitude of the atoms.
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© The Crystallographic Society of Japan
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