The Journal of the Japanese Society for Dental Materials and Devices
Online ISSN : 2188-4188
Print ISSN : 0286-5858
ISSN-L : 0286-5858
Original Article
Dentin Bonding of PMMA/MMA Resin Using Barbituric Acid Initiator System : Influence of Primer and Conditioning
Yorimitsu HOUGAYohji IMAI
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JOURNAL FREE ACCESS

1999 Volume 18 Issue 5 Pages 390-394

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Abstract
The influences of primers and dentin conditioning on bond strength of PMMA/MMA resin to dentin were studied using an initiator system consisting of barbituric acid, copper salt and quaternary ammonium chloride. While N-(2-methacryloxythyl)-2-pyrrolidone primer produced higher bond strength than HEMA primer, HEMA primer containing glutaraldehyde (Gluma) gave the highest bond strength. Pretreating dentin with 10% phosphoric acid containing 3% copper chloride (10 P-3 Cu) for 30s followed by rinsing with water for 30s produced significantly higher bond strength than the same conditioning for 10 s each regimen. The highest bond strength to dentin of PMMA/MMA resin, formulated with 2% 1-cyclohexyl-5-ethylbarbituric acid, 0.003% copper acetyl acetonate and 0.06% vinylbenzyltetradecyldimethylammonium chloride, was obtained after pretreating dentin with 10P-3Cu for 30 s and rinsing with water for 30 s followed by application of Gluma.
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© 1999 The Japanese Society for Dental Materials and Devices
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