The Journal of the Japanese Society for Dental Materials and Devices
Online ISSN : 2188-4188
Print ISSN : 0286-5858
ISSN-L : 0286-5858
Original Article
A Qualitative and Quantitative Analysis of the Extracts from Cured Composite Resins by HPLC : Part 1 Two paste type composite resins
Koji MIYAZAKITakashi HORIBEYoshifumi MIZUKAMIHiroshi INOUE
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JOURNAL FREE ACCESS

1983 Volume 2 Issue 1 Pages 8-17

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Abstract
 The low molecular components were contained in cured composite restorative resin, those materials were influenced to the chemical stabilities and the mechanical properties of cured resin.Therefore, we have been investigated on the extracts from cured composite restorative resins(Clearfil, Silar, Isopast)dipped into MeOH and H2O by using HPLC(High Performance Liquid Chromatography).
 The results were obtained as follows;
(1) The components were characterized in the extracts from cured composite resins that dipped into MeOH were as follows;
Clearfil:15 kinds, Silar:11 kinds, Isopast:11 kinds Ten kinds in those components were identified, such as TEGDMA, Bis-GMA, UDMA, GMA, DBP, BPO, TDEA, BA, BPA and Bis-GMA intermediate.
(2) The main components in the extracts from cured composite resins that dipped into MeOH were the monomers(TEGDMA, Bis-GMA, UDMA, Bis-GMA intermediate)and a plasticizer(DBP).
(3) Five or eight kinds of the components were charcterized in the extracts from cured composite resins that dipped into H2O, and the nine kinds in those components were identified.The solubilities of those components into H2O are probably as follows;
TEGDMA>GMA, TDEA>BA, Bis-GMA intermediate, BPA>Bis-GMA, UDMA, DBP>BPO.
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© 1983 The Japanese Society for Dental Materials and Devices
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