Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Paper
A Proposal of Recycling Type Spin-spray Ferrite Plating to Attain Low Environmental Load
Asako TakeuchiKen-ichi KatsumataKiyoshi OkadaNobuhiro Matsushita
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JOURNAL OPEN ACCESS

2011 Volume 58 Issue 9 Pages 560-565

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Abstract
A new-type ferrite plating process using recycled waste solution was proposed in this study to attain ferrite film fabrication at low environmental load. Although spin-spray technique enables us to deposit crystallized spinel ferrite films at very low temperature (<100°C) by spraying an aqueous reaction solution and oxidizing one onto substrates, this technique exhausts large quantity of waste solution, and it detracts the point of merit of ferrite plating as eco-friendly process. In this study, the waste solution, from which iron ions were removed as precipitated iron hydroxides, was used as recycled oxidizing solution in spin-spray technique. The additional amounts of oxidizer (H2O2) and pH modifier (NH3 aq) to waste solution significantly affected to the crystallinity and saturation magnetization of ferrite films fabricated by recycling process. The recycled oxidizing solution was prepared by adding relatively small amount 0.8 ml of H2O2 to waste solution of 3.0 L and adjusting the pH at relatively high 8.8-9.0. The ferrite films fabricated by using this recycled oxidizing solution had crystallite orientation and exhibited the saturation magnetization almost same as those of ferrite films fabricated by conventional spin-spray technique using fresh solutions.
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© 2011 by Japan Society of Powder and Powder Metallurgy

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