Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Effects of Dry Grinding on the Calcination of Oxide Superconductor YBa2Cu3O7-x
Yoshikazu Sadahiro
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JOURNAL OPEN ACCESS

1989 Volume 36 Issue 5 Pages 497-500

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Abstract
The mixture of Y2O3, BaCO3 and CuO was ground by a vibration mill with allumina vessel.The products were calcined at 925°C for 2 days, and annealed at 500°C for several days. The effects of dry grinding on the samples were inferred from the variations of the strain (<ε I.2>1/2 ) and the lattice parameters (a, bc) determined by X-ray diffraction.
As the results, it has been clarified that the grinding for 100 minutes under above mentioned heating conditions gives the best conductor of these products.
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