Abstract
We examined the structures of (110) preferred oriented YBa2Cu3Oy thin films by X-ray diffractometry with a 4-axis goniometer. It is noted that some films, in which the RHEED method had detected only the (110) domain, had (103) domains. The results indicate that the films have different structures between their surface and inside. So to characterize the precise structure of the films, this X-ray diffraction method is very useful.