Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Preparation of MoSi2-x(X=B, Al, Nb)Alloys by MA-PDS Process
Manabu MatsubaraHitoshi HashimotoYong-Ho Park
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JOURNAL OPEN ACCESS

2000 Volume 47 Issue 11 Pages 1150-1155

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Abstract
In order to improve the mechanical properties of MoSi2 alloys, the alloys with Al, B or Nb addition were prepared by an advanced consolidation process which combined mechanical alloying with pulse discharge sintering (MA-PDS). Their microstructure and mechanical properties were investigated. The MoSi2 alloys fabricated by MA-PDS process showed very fine microstructure when compared with the sample sintered from commercial MoSi2 powder. The sintered alloys made from powder milled in Ar atmosphere had dense microstructure compared with that milled in air because of suppression of oxide formation during milling, except for Al added alloy. On the effect of added elements in densification of the alloys, addition of B was more effective than Al or Nb. Both in the Vickers hardness test and in the tensile test at ambient temperature, the alloys fabricated by MA-PDS process showed good performance compared with the sample sintered from commercial MoSi2 powder due to the fine grain.
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