Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Examination of Crystal Orientation in Green Compact and Sintered Nd-Fe-B Magnets by X-ray Diffraction
Shigeru TakakiKen MakitaAtsuki Okamoto
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JOURNAL OPEN ACCESS

2003 Volume 50 Issue 1 Pages 45-49

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Abstract
In order to investigate the texture formation of Nd-Fe-B system sintered magnet, 006 Miller indices pole figures of (Nd⋅Dy)2Fe14B phase were measured for as-compacted sample and for as-sintered one by X-ray diffraction. The degree of preferred orientation P was estimated by the integration of the product between the normalized diffraction intensity IN and cosα, which α is the inclined angle between the direction of the applied magnetic field and that of the magnetic moment in each grain. As a result, P had good corelation with the remanence Br in sintered sample. P in as-compacted sample was always lower than that in as-sintered one. The difference between as-sintered state and as-compacted state was largest when the magnetic field was 0.2T.
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