Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Hydrothermal Synthesis of Nano Sized Oxided Particles
Yuko SawakiKazutaka MatsuoMikio Kishimoto
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JOURNAL OPEN ACCESS

2003 Volume 50 Issue 10 Pages 787-791

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Abstract
We synthesized nano sized cerium and zirconium oxide particles by the hydrothermal treatment of precipitates formed from the chlorides of each metal ion. Especially the cerium oxide particles had plate-like shapes with the particle size in the range of 2-20 run. Even in the particle size of 2nm, most of the cerium oxide particles observed by a high resolution transmission electron microscope showed clear lattice images based on (111) and (200) planes indicating the plate-like single crystals. In the zirconium oxide particles, it was confirmed that the single phases of monoclinic and tetragonal crystals were obtained by the hydrothermal treatment lower than 200°C maintaining the particle size of about 10nm.
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