Journal of Advanced Science
Online ISSN : 1881-3917
Print ISSN : 0915-5651
ISSN-L : 0915-5651
Preparation of lead-zirconiate-titanate using lead acetate by a sol-gel process
Yoichi ISHIMOTONozomi IMAHORIJun-ichi MATSUSHITA
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1999 Volume 11 Issue 1 Pages 67-68

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Abstract
Lead-zirconate-titanate (PZT) was prepared by a sol-gel process. As one process, lead acetate, zirconium tetra-n-butoxide, and titanium tetra-iso-propoxide were used as raw materials. 2-methoxyethanol and diethanolamine were used as solvents. As another process, lead acetate, zirconyl nitrate, and titanium tetra-n-butoxide were used as raw materials. Distilled water, acetic acid, and tri-ethylene glycol were used as solvents. PZT were synthesized twelve ways on the basics to the two processes. Synthesized PZT by each had been dried for 24h at 338K. Dried samples had been sintered for 1h at 773K, 873K, and 1023K in air. The sintered samples were evaluated by X-ray analysis.
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