Netsu Sokutei
Online ISSN : 1884-1899
Print ISSN : 0386-2615
ISSN-L : 0386-2615
Measurement of High Temperature Heat Content by Drop Calorimetry
Katsunori YamaguchiKimio Itagaki
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2002 Volume 29 Issue 4 Pages 173-180

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Abstract
Accurate data for high temperature heat contents and heat capacities of substances are valuable for the study of materials and processes at elevated temperature. The heat contents and heat capacities of solids and liquids above 1000K are determined experimentally by drop calorimetry and the use has been extended to higher temperatures by using modern techniques for measuring and controlling temperature. The general requirements for the drop method are described in terms of furnace assembly, temperature measurement, calorimeter and sample container. Heat capacities can be determined from relative heat content measurements. Shomate function and qusai-local linear regression (QLLR) are useful to accurately derive the heat capacities from the heat contents. Several applications of the heat content measurements are described.
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© Japan Society of Calorimetry and Thermal Analysis
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