The Proceedings of Conference of Kansai Branch
Online ISSN : 2424-2756
2025.100
Session ID : 20610
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Effect of Grain Refinement on the Pitting Corrosion Resistance of Fe-12Cr Steel
*Futoshi WAKIHiroyuki MIYAMOTOMotohiro YUASA
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Abstract

With industrial advancements, aerospace, energy, and medical fields demand stronger, more durable, and lightweight materials. Ultrafine-grained (UFG) structures, achieved through severe plastic deformation (SPD) techniques like Equal-Channel Angular Pressing (ECAP), enhance mechanical properties and corrosion resistance. However, literature on UFG effects on corrosion resistance remains inconsistent, likely due to microstructural complexity. In this study, Fe-12Cr alloy underwent ECAP (8 passes) for grain refinement. Dislocation density was evaluated using X-ray diffraction and the Williamson-Hall method, and low-temperature heat treatment was applied to selectively reduce dislocations without grain growth. EBSD confirmed grain sizes of 30–50 nm. Despite refined grains, heat-treated samples showed decreased pitting corrosion resistance. The results suggest that dislocation density plays a crucial role in corrosion resistance, indicating that grain refinement alone is insufficient, and residual dislocations are key to improving corrosion resistance.

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© 2025 The Japan Society of Mechanical Engineers
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