The Proceedings of the Materials and Mechanics Conference
Online ISSN : 2424-2845
2018
Session ID : GS0704
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In situ FESEM fracture toughness experiment of copper nano-films with controlled surface oxide layer
*Toshiyuki KONDODaiki MIKIHiroyuki HIRAKATAKohji MINOSHIMA
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Abstract

The purpose of this study is to clarify the effects of surface oxide layer on fracture toughness of approximately 500-nm-thick freestanding copper nano-films. Freestanding film specimens with thermal oxide layer (oxide layer thickness: ~3 nm and ~6 nm) were prepared by thermal treatment in dry air. Specimens without oxide layer were prepared by removing the surface oxide layer by means of argon ion sputtering. In situ field emission scanning electron microscope fracture toughness experiments confirmed that a crack initiated at the notch root by applying a tensile load. The effects of surface oxide layer on the critical crack tip opening displacement of the specimens with native/thermal oxide layer were not clearly observed. On the other hand, the critical crack tip opening displacement of the specimens without oxide layer was clearly higher than that of the specimens with native/thermal oxide layer.

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© 2018 The Japan Society of Mechanical Engineers
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