Papers in Meteorology and Geophysics
Online ISSN : 1880-6643
Print ISSN : 0031-126X
ISSN-L : 0031-126X
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Determination of Halogenated Hydrocarbons in the Air by Cryogenic Preconcentration and Gas Chromatography-Quadrupole Mass Spectrometry
Katsuhiko FushimiYukio Sugimura
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1981 Volume 32 Issue 4 Pages 313-316

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Abstract
   A simple method is described for the preconcentration and determination of some of the atmospheric chlorofluorocarbons by using the GC-QMS method. The halogenated hydrocarbons in 100 ml of air sample were preconcentrated into 1.7 ml of cold trap by using helium stream and were injected into a GC column. The determination of F-11 and F-12 was done by electron impact mode of the GC-QMS method. Recovery of this method is 100% and the results of replicate determinations are in good agreement with each other within the analytical error.
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© 1981 by Japan Meteorological Agency / Meteorological Research Institute
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