1985 Volume 1985 Issue 6 Pages 1121-1123
Silicon nitride powders of α- and β-types were activated by vibration ball milling, and the mechanochemical activation has been investigated by means of X-ray diffractometry and calorimetry. The specific surface area of two types of ground Si3N4 powders increased monotonically with the increase of grinding time. The fine grinding promoted the fragmentation of crystallites and an increase of lattice strain particularly in β-type. The surface energy of ground Si3N4 powders increased remarkably.
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