Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
17th Fall Meeting of The Ceramic Society of Japan
Session ID : 3B02
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Host: The Ceramic Society of Japan

Nano Indentation Rheology of Phenil Group-Containing Sol-Gel Hybrid Films
Motomu Sasaki, Hiroyuki Muto, Atsunori Matsuda, *Mototsugu Sakai
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Keywords: Nano-Indentation, Sol/gel-derived film, Viscoelastic analysis, Stress relaxation, Polyphenylsilsesquioxane
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Abstract
Nano-indentation tests with a Berkovich diamond indenter are conducted for examining the gelling process of polyphenylsilsesquioxane hybrid films. A mathematical algorithm is formulated for quantitatively analyzing the indentation-generated stress-relaxation data. The viscoelastic functions of the films are, then, correlated to the microstructural evolution in the gelling process.
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© The Ceramic Society of Japan 2004
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