Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
Preprints of Annual Meeting of The Ceramic Society of Japan, 2004
Session ID : 1F28
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Host: The Ceramic Society of Japan

Synthesis of Methoxy-modified Octosilicate
*Shosuke Kiba, Shintaro Watanabe, Kazuyuki Kuroda
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Keywords: Layered Polysilicate, Inorganic-organic Hybrid, esterification, Intercalation
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Abstract
Layered polysilicate octosilicate (Na8[Si32O64(OH)8‚32H2O], Na-Oct) was modified with methanol as a course of our study on nanoscaled inorganic-organic hybrids. The interlayer sodium ions were exchanged with protons by acid treatment and the H-type octosilicate was allowed to reat with methanol to form methoxy-modified octosilicate. The immobilization of methoxy groups onto the interlayer silanol groups was confirmed by XRD, 13C CP/MAS NMR,and TG-DTA.
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© The Ceramic Society of Japan 2004
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