Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
24th Fall Meeting of The Ceramic Society of Japan
Session ID : 1O20
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Microstructure of TiN-TiB2 Composites Prepared by Spark Plasma Sintering and Arc Melting
*Mettaya KitiwanAkihiko ItoTakashi Goto
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Abstract
Non-oxide ceramic materials like titanium nitride (TiN) and titanium boride (TiB2) have become a promising candidate for advanced structural materials due to theirs excellent mechanical strength and chemical stability at elevated temperature. This work attempts to study the sintering of TiN-TiB2 composite by spark plasma sintering (SPS); the arc melting was also performed to investigate the morphology of specimen. The mixing powders of various compositions were densified at 2173-2573 K under the pressure of 10 MPa for 60-300 s. The density over 99%TD was achieved for composite with the TiB2 content of 20-40vol% sintered at 2573 K under the pressure of 10 MPa for 60 s. While the TiN-TiB2 prepared by SPS showed the core-shell structure, the composite obtained by arc melting had the eutectic structure.
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© The Ceramic Society of Japan 2011
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