Precise Raman measurements of C60 fullerene nanowhiskers synthesized using the liquid-liquid interfacial precipitation method

Toshio Konno; Chika Hirata; Erlon Henrique Martins Ferreira; Lingling Ren; Guangzhe Piao; José Manuel Juárez García; Froy Martínez Suárez; Sergio Joaquín Jiménez Sandoval; Takatsugu Wakahara; Kun’ichi Miyazawa

doi:10.14723/tmrsj.41.289

Regular Papers

Precise Raman measurements of C₆₀ fullerene nanowhiskers synthesized using the liquid-liquid interfacial precipitation method

Toshio Konno, Chika Hirata, Erlon Henrique Martins Ferreira, Lingling Ren, Guangzhe Piao, José Manuel Juárez García, Froy Martínez Suárez, Sergio Joaquín Jiménez Sandoval, Takatsugu Wakahara, Kun’ichi Miyazawa

Author information

Toshio Konno
Fullerene Engineering Group, Materials Processing Unit, National Institute for Materials Science (NIMS)
Chika Hirata
Fullerene Engineering Group, Materials Processing Unit, National Institute for Materials Science (NIMS)
Erlon Henrique Martins Ferreira
National Institute of Metrology, Quality and Technology (INMETRO)
Lingling Ren
National Institute of Metrology (NIM)
Guangzhe Piao
Qingdao University of Science and Technology (QUST)
José Manuel Juárez García
National Center of Metrology (CENAM)
Froy Martínez Suárez
Centro de Investigación y Estudios Avanzados del Instituto Politecnico Nacional (CINVESTAV)
Sergio Joaquín Jiménez Sandoval
Centro de Investigación y Estudios Avanzados del Instituto Politecnico Nacional (CINVESTAV)
Takatsugu Wakahara
Fullerene Engineering Group, Materials Processing Unit, National Institute for Materials Science (NIMS)
Kun’ichi Miyazawa
Fullerene Engineering Group, Materials Processing Unit, National Institute for Materials Science (NIMS)

Keywords: Fullerene nanowhisker, C₆₀, Fullerene, LLIP, Raman spectrometry

JOURNAL FREE ACCESS

2016 Volume 41 Issue 3 Pages 289-295

DOI https://doi.org/10.14723/tmrsj.41.289

Details

Abstract

Raman measurements and uncertainty evaluations were conducted for C₆₀ fullerene nanowhiskers (C₆₀FNWs) synthesized using the liquid-liquid interfacial precipitation (LLIP) method and for a vacuum-deposited C₆₀ thin film. No photopolymerization was observed for the C₆₀ molecules when the specimens were irradiated by a green laser of 532 nm wavelength at a power density of 5.7×10³ mW/mm². It is demonstrated that the 1469.95 ± 0.42 cm^-1 can be used as a standard peak position of the A_g(2) mode of C₆₀FNWs.

Corresponding author

Register with J-STAGE for free!