X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 7
Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one
Thippeswamy G. B., Vijaykumar D., Prasad T. N. Mahadeva, Jayashree B. S., Lakshminarayana B. N., Sridhar M. A., Prasad J. Shashidhara
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Supplementary material

2011 Volume 27 Pages 39-40

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Abstract
The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å, c = 13.4990(18)Å, α = 68.808(4)°, β = 81.149(7)°, γ = 79.863(7)°, V = 1511.5(3)° and Z = 4. In the crystal, O-H…O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2σ(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.
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© 2011 by The Japan Society for Analytical Chemistry
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