Synthesis and Crystal Structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

T. N. Mahadeva PRASAD; S. L. GAONKAR; Kamini. KAPOOR; Vivek. K. GUPTA; Rajnikant; H. SHIMIZU; M. A. SRIDHAR; J. Shashidhara PRASAD

doi:10.2116/xraystruct.28.25

Part 4

Synthesis and Crystal Structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

T. N. Mahadeva PRASAD, S. L. GAONKAR, Kamini. KAPOOR, Vivek. K. GUPTA, Rajnikant, H. SHIMIZU, M. A. SRIDHAR, J. Shashidhara PRASAD

Author information

T. N. Mahadeva PRASAD
Department of Studies in Physics, University of Mysore
S. L. GAONKAR
Department of Chemistry, Manipal Institute of Technology
Molecular and Biological Technology Research group, Bioproductuin Research Institute, National Institute of Advanced Industrial Science and Technology (AIST)
Kamini. KAPOOR
X-ray Crystallography Laboratory, Post-Graduate Department of Physics, University of Jammu
Vivek. K. GUPTA
X-ray Crystallography Laboratory, Post-Graduate Department of Physics, University of Jammu
Rajnikant
X-ray Crystallography Laboratory, Post-Graduate Department of Physics, University of Jammu
H. SHIMIZU
Molecular and Biological Technology Research group, Bioproductuin Research Institute, National Institute of Advanced Industrial Science and Technology (AIST)
M. A. SRIDHAR
Department of Studies in Physics, University of Mysore
J. Shashidhara PRASAD
Sri Sathya Sai Institute of Higher Learning

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Supplementary material

2012 Volume 28 Pages 25-26

DOI https://doi.org/10.2116/xraystruct.28.25

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Abstract

The title compound, C₁₅H₁₇N₃O₂, was synthesized, and the structure was characterised spectroscopically by ¹H NMR and ¹³C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group P1 with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675 Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å³.

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