X-ray Structure Analysis Online
Online ISSN : 1883-3578
Part 5
Synthesis and Crystal Structure of 1-p-Tolyl-3-(3-(trifluoromethyl)phenyl)-triaz-1-ene 1-oxide
Behrooz REZAEILadan NIROMANDKamal ALIZADEHPascal RETAILLEAU
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Volume 28 (2012) Pages 37-38

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Abstract

The crystal structure of 1-p-tolyl-3-(3-(trifluoromethyl)phenyl)triaz-1-ene 1-oxide is triclinic, space group P1 with a = 6.065(2), b = 8.391(2), c = 13.529(3)Å, α = 82.047(5), β = 84.350(5), γ = 83.377(5)°, and Z = 2. The crystal structure was solved by direct methods, and refined by full-matrix least squares to final values of R1 = 0.0579 and wR2 = 0.1453 with 2000 reflections (I > 2σ(I)). There are intermolecular hydrogen bonds between the NH groups acting, as donors and O atoms as acceptors and F…F interactions.

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© 2012 by The Japan Society for Analytical Chemistry
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