Crystal Structure of 4-Hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone

Adriano Bof de OLIVEIRA; Johannes BECK; Jörg DANIELS; Bárbara Regina Santos FEITOSA

doi:10.2116/xraystruct.31.5

X-ray Structure Analysis Online

Online ISSN : 1883-3578
ISSN-L : 1883-3578

Part 1

Crystal Structure of 4-Hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone

Adriano Bof de OLIVEIRA, Johannes BECK, Jörg DANIELS, Bárbara Regina Santos FEITOSA

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Supplementary material

2015 Volume 31 Pages 5-6

DOI https://doi.org/10.2116/xraystruct.31.5

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Abstract

The structure of 4-hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone (VAMTSC) was determined by X-ray crystallography. The molecular structure matches the asymmetric unit, and the compound crystallizes in a monoclinic system. It was characterized thus: P2₁/c, a = 8.4960(3), b = 8.5040(2), c = 17.2236(6)Å, β = 111.513(2)°, Z = 4, V = 1157.71(6)Å³. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F² to final values of R1 = 0.0403 and wR2 = 0.078.

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