X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 4
Crystal Structure of cis-Bis(2,2′-bipyridyl)bis(trifluoromethanesulfonato)cobalt(II)
Mari TOYAMAYu YAMAMOTO
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2019 Volume 35 Pages 21-23

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Abstract

A cobalt(II) complex with two 2,2′-bipyridine (bpy) and two trifluoromethanesulfonato (OTf) ligands, cis-[CoII(OTf )2(bpy)2], was prepared, and the crystal structure at 173 K was elucidated by the single-crystal X-ray diffraction method. The complex crystallized in the monoclinic space group C2/c with a = 9.90587(16), b = 14.2978(2), c = 18.6626(3)Å, α = 90, β = 101.6670(17), γ = 90°, Z = 4, V = 2588.61(7)Å3. The R1 and wR2 values were 0.0397 and 0.1016, respectively, for 2377 reflections.

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© 2019 by The Japan Society for Analytical Chemistry
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