Crystal Structure of (Z)-4-[4-Fluorophenyl]thiosemicarbazide4

Uwaisulqarni M. OSMAN; Sharmili SILVARAJOO; Irshad Ul Haq BHAT; Mohd Hasmizam RAZALI; Mohd Zul Helmi ROZAINI; Thahira Begum S. A. RAVOOF

doi:10.2116/xraystruct.36.49

Part 12

Crystal Structure of (Z)-4-[4-Fluorophenyl]thiosemicarbazide⁴

Uwaisulqarni M. OSMAN, Sharmili SILVARAJOO, Irshad Ul Haq BHAT, Mohd Hasmizam RAZALI, Mohd Zul Helmi ROZAINI, Thahira Begum S. A. RAVOOF

Author information

JOURNAL FREE ACCESS
Supplementary material

2020 Volume 36 Pages 49-50

DOI https://doi.org/10.2116/xraystruct.36.49

Details

Abstract

The present compound, namely (Z)-4-[4-fluorophenyl]thiosemicarbazide, crystallized in a monoclinic space group, P2₁/c, with cell parameters a = 12.1056(8)Å, b = 5.5177(4)Å, c = 12.5617(8)Å, β = 90.063(2)°, V = 839.06(10)Å³, and Z = 4. The structure was solved and the data was refined to reach R and wR indices of 0.0946 and 0.1377, respectively. In the crystal, each molecule was linked to the next molecule by two N–H···S intermolecular hydrogen bonds.

Corresponding author

Register with J-STAGE for free!