On-Line Sample Enrichment and Cleanup for High Performance Liquid Chromatography with Column Switching Technique A Review

Hideo IMAI; Gen TAMAI; Tsutomu MASUJIMA; Ikue MORITA-WADA

doi:10.2116/analsci.5.389

Hideo IMAI, Gen TAMAI, Tsutomu MASUJIMA, Ikue MORITA-WADA

Author information

Keywords: High performance liquid chromatography, column switching, solid extraction, drug analysis, on-line deproteinization, biological samples

JOURNAL FREE ACCESS

1989 Volume 5 Issue 4 Pages 389-393

DOI https://doi.org/10.2116/analsci.5.389

Details

Published: August 10, 1989 Received: January 17, 1989 Available on J-STAGE: June 30, 2006 Accepted: April 20, 1989 Advance online publication: - Revised: -
Correction information
Date of correction: June 30, 2006 Reason for correction: - Correction: CITATION Details: Wrong : 1). B. L. Karger, R. W. Giese and L. R. Snyder, TRAC, 2, 106 (1983).
2). J. F. K. Huber, R. Van der Linden, E. Ecker and M. Orleans, J. Chromatogr., 83, 267 (1973).
3). F. F. Cantwell, Anal. Chem., 48, 1854 (1976).
4). R. J. Dolphin, F. W. Willmott, A. D. Mills and L. P. J. Hoogeveen, J. Chromatogr., 122, 259 (1976).
5). F. W. Willmott, I. Mackenzie and R. Dolphin, J. Chromatogr., 167, 31(1978).
6). F. Erni and R. W. Frei, J. Chromatogr., 149, 561 (1978).
7). A. Nazareth, L. Jaramillo, B. L. Karger, R. W. Giese and L. R. Snyder, J. Chromatogr., 309, 357 (1984).
8). K. A. Ramsteiner, J. Chromatogr., 456, 3 (1988). 3939.
9). J. F. K. Huber, J. A. R. J. Hulsman and C. A. M. Meijers, J. Chromatogr., 62, 79 (1971).
10). B. L. Karger, M. Martin and G. Guichon, Anal. Chem., 46, 1640 (1974).
11). J. N. Little and G. J. Fallick, J. Chromatogr., 112, 389 (1975).
12). P. Schauwecker, R. W. Frei and F. Erni, J. Chromatogr., 136, 63 (1977).
13). J. F. K. Huber and R. R. Becker, J. Chromatogr., 142, 765 (1977).
14). J. Lankelma and H. Poppe, J. Chromatogr., 149, 587 (1978).
15). D. D. Koch and P. T. Kissinger, Anal. Chem., 52, 27 (1980).
16). J. C. Gfeller and M. Stockmeyer, J. Chromatogr., 198, 162 (1980).
17). A. D. Blair, A. W. Forrey, B. T. Meijsen and R. E. Culture, J. Pharm. Sci., 63, 1334 (1975).
18). G. J. DeJong, J. Chromatogr., 183, 203 (1980).
19). W. Roth, K. Beschke, R. Jauch, A. Zimmer and F. W. Koss, J. Chromatogr., 222, 13 (1981).
20). C. E. Werkhoven-Goewie, U. A. Th. Brinkman and R. W. Frei, Anal. Chem., 53, 2072 (1981).
21). R. A. Hux, H. Y. Mohammad and F. F. Cantwell, Anal. Chem., 54, 113 (1982).
22). H. Yoshida, I. Morita, T. Masujima and H. Imai, Chem. Pharm. Bull., 30, 2287 (1982).
23). H. Yoshida, I. Morita, T. Masujima and H. Imai, Chem. Pharm. Bull., 30, 3827 (1982).
24). T. Arvidsson, J. Chromatogr., 439, 353 (1988).
25). R. Wyss and F. Bucheli, J. Chromatogr., 456, 33 (1988).
26). H. Yoshida, I. Morita, G. Tamai, T. Masujima, T. Tsuru, N. Takai and H. Imai, Chromatographia, 19, 466 (1984).
27). H. Imai, H. Yoshida, T. Masujima, I. Morita, K. Matsuura, A. Nakamaru, K. Katayama and H. Matsuo, Anal. Lett.,16, 1109 (1983).
28). H. Yoshida, K. Takano, I. Morita, T. Masujima and H. Imai, Jap. J. Clin. Chem., 12, 312 (1983).
29). G. Tamai, I. Morita, T. Masujima, H. Yoshida and H. Imai, J. Pharm. Sci., 73, 1825 (1984).
30). G. Tamai, H. Yoshida, H. Imai, T. Takashina, K. Kotoo, T. Fuwa, Y. Tsuchioka, H. Matsuura and G. Kajiyama,Chromatographia, 20, 671 (1985).
31). I. Morita, T. Masujima, H. Yoshida and H. Imai, Bunseki Kagaku, 33, E235 (1984).
32). I. Morita, T. Masujima, H. Yoshida and H. Imai, Anal. Biochem., 151, 358 (1985).
33). T. Dohji, M. Fushimi, T. Kawabe and F. Kamiyama, J. Chromatogr., 311, 249 (1984).
34). S. Hasegawa, R. Uenoyama, F. Takeda, J. Chuma, K. Suzuki, F. Kamiyama, K. Yamazaki and S. Baba, J. Liq. Chromatogr., 7, 2267 (1984).
35). H. Kitamura, M. Hayashi, H. Mikami and Y. Ishida, Bunseki Kagaku, 35, 358 (1986).
36). I. H. Hagestam and T. C. Pinkerton, Anal. Chem., 57, 1757 (1985).
37). H. Takahagi, K. Inoue and M. Horiguchi, J. Chromatogr., 352, 369 (1986).
38). H. Imai, G. Tamai and S. Sakura, J. Chromatogr., 371, 29 (1986).
39). G. Tamai, H. Yoshida and H. Imai, Bunseki Kagaku, 35, 236 (1986).
40). G. Tamai, H. Imai and H. Yoshida, Chromatographia, 21, 519 (1986).
41). G. Tamai, H. Yoshida and H. Imai, Anal. Sci., 2, 481 (1986).
42). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 155 (1987).
43). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 147 (1987).
44). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 163 (1987).
45). H. Imai and G. Tamai, Biomed. Chromatogr., in press.

Right : 1). B. L. Karger, R. W. Giese and L. R. Snyder, TRAC, 2, 106 (1983).
2). J. F. K. Huber, R. Van der Linden, E. Ecker and M. Orleans, J. Chromatogr., 83, 267 (1973).
3). F. F. Cantwell, Anal. Chem., 48, 1854 (1976).
4). R. J. Dolphin, F. W. Willmott, A. D. Mills and L. P. J. Hoogeveen, J. Chromatogr., 122, 259 (1976).
5). F. W. Willmott, I. Mackenzie and R. Dolphin, J. Chromatogr., 167, 31(1978).
6). F. Erni and R. W. Frei, J. Chromatogr., 149, 561 (1978).
7). A. Nazareth, L. Jaramillo, B. L. Karger, R. W. Giese and L. R. Snyder, J. Chromatogr., 309, 357 (1984).
8). K. A. Ramsteiner, J. Chromatogr., 456, 3 (1988).
9). J. F. K. Huber, J. A. R. J. Hulsman and C. A. M. Meijers, J. Chromatogr., 62, 79 (1971).
10). B. L. Karger, M. Martin and G. Guichon, Anal. Chem., 46, 1640 (1974).
11). J. N. Little and G. J. Fallick, J. Chromatogr., 112, 389 (1975).
12). P. Schauwecker, R. W. Frei and F. Erni, J. Chromatogr., 136, 63 (1977).
13). J. F. K. Huber and R. R. Becker, J. Chromatogr., 142, 765 (1977).
14). J. Lankelma and H. Poppe, J. Chromatogr., 149, 587 (1978).
15). D. D. Koch and P. T. Kissinger, Anal. Chem., 52, 27 (1980).
16). J. C. Gfeller and M. Stockmeyer, J. Chromatogr., 198, 162 (1980).
17). A. D. Blair, A. W. Forrey, B. T. Meijsen and R. E. Culture, J. Pharm. Sci., 63, 1334 (1975).
18). G. J. DeJong, J. Chromatogr., 183, 203 (1980).
19). W. Roth, K. Beschke, R. Jauch, A. Zimmer and F. W. Koss, J. Chromatogr., 222, 13 (1981).
20). C. E. Werkhoven-Goewie, U. A. Th. Brinkman and R. W. Frei, Anal. Chem., 53, 2072 (1981).
21). R. A. Hux, H. Y. Mohammad and F. F. Cantwell, Anal. Chem., 54, 113 (1982).
22). H. Yoshida, I. Morita, T. Masujima and H. Imai, Chem. Pharm. Bull., 30, 2287 (1982).
23). H. Yoshida, I. Morita, T. Masujima and H. Imai, Chem. Pharm. Bull., 30, 3827 (1982).
24). T. Arvidsson, J. Chromatogr., 439, 353 (1988).
25). R. Wyss and F. Bucheli, J. Chromatogr., 456, 33 (1988).
26). H. Yoshida, I. Morita, G. Tamai, T. Masujima, T. Tsuru, N. Takai and H. Imai, Chromatographia, 19, 466 (1984).
27). H. Imai, H. Yoshida, T. Masujima, I. Morita, K. Matsuura, A. Nakamaru, K. Katayama and H. Matsuo, Anal. Lett.,16, 1109 (1983).
28). H. Yoshida, K. Takano, I. Morita, T. Masujima and H. Imai, Jap. J. Clin. Chem., 12, 312 (1983).
29). G. Tamai, I. Morita, T. Masujima, H. Yoshida and H. Imai, J. Pharm. Sci., 73, 1825 (1984).
30). G. Tamai, H. Yoshida, H. Imai, T. Takashina, K. Kotoo, T. Fuwa, Y. Tsuchioka, H. Matsuura and G. Kajiyama,Chromatographia, 20, 671 (1985).
31). I. Morita, T. Masujima, H. Yoshida and H. Imai, Bunseki Kagaku, 33, E235 (1984).
32). I. Morita, T. Masujima, H. Yoshida and H. Imai, Anal. Biochem., 151, 358 (1985).
33). T. Dohji, M. Fushimi, T. Kawabe and F. Kamiyama, J. Chromatogr., 311, 249 (1984).
34). S. Hasegawa, R. Uenoyama, F. Takeda, J. Chuma, K. Suzuki, F. Kamiyama, K. Yamazaki and S. Baba, J. Liq. Chromatogr., 7, 2267 (1984).
35). H. Kitamura, M. Hayashi, H. Mikami and Y. Ishida, Bunseki Kagaku, 35, 358 (1986).
36). I. H. Hagestam and T. C. Pinkerton, Anal. Chem., 57, 1757 (1985).
37). H. Takahagi, K. Inoue and M. Horiguchi, J. Chromatogr., 352, 369 (1986).
38). H. Imai, G. Tamai and S. Sakura, J. Chromatogr., 371, 29 (1986).
39). G. Tamai, H. Yoshida and H. Imai, Bunseki Kagaku, 35, 236 (1986).
40). G. Tamai, H. Imai and H. Yoshida, Chromatographia, 21, 519 (1986).
41). G. Tamai, H. Yoshida and H. Imai, Anal. Sci., 2, 481 (1986).
42). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 155 (1987).
43). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 147 (1987).
44). G. Tamai, H. Yoshida and H. Imai, J. Chromatogr., 423, 163 (1987).
45). H. Imai and G. Tamai, Biomed. Chromatogr., in press.

Date of correction: June 30, 2006 Reason for correction: - Correction: PDF FILE Details: -

Abstract

The usability of column-switching techniques of high performance liquid chromatography is reviewed with special interest given to the enrichment and cleanup of biological samples. In Section 2, band broadening and a fully automated operation system are especially noted. In Sections 3 and 4, it is emphasized that the recovery of on-line solid extraction in a precolumn is quantitative (100%), depending upon the combination of the stationary phase and the mobile phase. In Section 5, are elucidated the deproteinization and recovery from protein-bound entities by a size exclusion coupled with internal-surface reversed-phase techniques or by hydrophobic interaction. These methods are extensively applied to the biological samples, such as whole blood and tissue homogenates, which contain minute particles, by using a large-bore endfitting filter for the precolumn.

Corresponding author

Correction information

Register with J-STAGE for free!