Journal of The Adhesion Society of Japan
Online ISSN : 2187-4816
Print ISSN : 0916-4812
ISSN-L : 0916-4812
Technical Report
Microencapsulation of Hardening Agent for Epoxy Resin by Interfacial Hardening Reaction Method
Yosuke SAKAIHiroshi YOKOYAMAYoshinari TAGUCHIMasato TANAKA
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2006 Volume 42 Issue 7 Pages 272-279

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Abstract
In order to apply to the one liquid type blocking adhesive, it was tried to microencapsulate the hardening agent for epoxy resin with epoxy resin by the interfacial hardening reaction method.In the experiment, the reaction time, the concentration of epoxy resin as the shell material and the impeller speed during the microencapsulation process were changed stepwise.It was investigated how these experimental conditions affect the structure, the gelation time and storage stability of microcapsules.It is found that the size, the content of hardening agent and the shell thickness of microcapsules could be controlled by changing the reaction time, the concentration of epoxy resin and the impeller speed.As a result, the storage stability and the gelation time of microcapsules were able to be changed widely.
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© 2006 The Adhesion Society of Japan
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