Journal of The Adhesion Society of Japan
Online ISSN : 2187-4816
Print ISSN : 0916-4812
ISSN-L : 0916-4812
Original Paper
Changes in Physical and Chemical Properties of Sucrose bythe Addition of Ammonium Dihydrogen Phosphate
Kenji UMEMURAShin HAYASHISoichi TANAKAKozo KANAYAMA
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2017 Volume 53 Issue 4 Pages 112-117

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Abstract

To explore the possibility of a novel natural wood adhesive, we clarified that the basic characteristicsof sucrose with added ammonium dihydrogen phosphate (ADP). Sucrose and ADP mixed at variousweight ratios were heated at 120-200℃ for a maximum of 20 min. Thermal analyses, insoluble matterrate against boiling water, and Fourier transform infrared spectroscopy (FT-IR) were measured.The thermal properties of sucrose lowered significantly with the addition of a small amount of ADP.The insoluble matter rate increased with increasing heating temperature, irrespective of mixture ratio.However, the addition of a large quantity of ADP resulted in a low insoluble matter rate. The effectiveheating time and ADP content at 180℃ were 10 min and 10wt%, respectively. The heated mixturecontained a furan ring and carbonyl group, according to the results of FT-IR. It was clarified that sucrosechanged to a high water-resistant substance by the addition of ADP and heating treatment.

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© 2017 The Adhesion Society of Japan
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