Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Original Papers
Simple Method for Determining Trace Pesticides in Air Using Extraction Disks
Hitoshi MURAYAMAHiroyuki MUKAIHideko MITOBENoboru MORIYAMA
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2000 Volume 16 Issue 3 Pages 257-263

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Abstract
A conventional method for the quantitative and simultaneous analysis of a large number of pesticides was proposed using a combination of commercial extraction disks and a quartz-fiber disk. Pesticides contained in air were collected on these disks at a flow rate of 10 l min-1 and extracted by acetone. The extracted solution was analyzed quantitatively with GC/MS. In order to evaluate the accuracy of this method, a recovery test was performed. Forty-five kinds of pesticides were spiked on the quartz-fiber disk at a concentration level of 0.2 μg by collecting 10 m3 of clean air. The recovery efficiencies of almost 40 kinds of pesticides showed more than 80%, and the coefficients of variations were less than 20%. The method was applied to a practical environmental analysis of pesticides, and an appropriate result could be obtained.
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© 2000 by The Japan Society for Analytical Chemistry
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