Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Notes
Comprehensive Analytical Method for Semi-volatile Organic Compounds in Water Samples by Combination of Disk-type Solid-phase Extraction and Gas Chromatography–Mass Spectrometry Database System
Daisuke JINYATomomi IWAMURAKiwao KADOKAMI
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Supplementary material

2013 Volume 29 Issue 4 Pages 483-486

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Abstract
A disk-type solid-phase extraction method for simultaneous extraction of a wide range of semi-volatile organic compounds in water samples was developed. The developed method could extract 186 out of 202 model compounds from spiked environmental samples (0.1 μg/L) with 94% average recovery (50 – 111%). Compared with the previous cartridge-type method, the extraction time was reduced to approximately 1/6. Applying the combination of the developed method and the database system to environmental samples for non-target analyses, 39 micro-pollutants with a wide range of physicochemical properties were determined.
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© 2013 by The Japan Society for Analytical Chemistry
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