Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Determination of Trace Amount of Lead in Natural Water by Isotope Dilution-Inductively Coupled Plasma Mass Spectrometry
Akihide ItohToru OzakiKoichi ChibaHiroki Haraguchi
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1997 Volume 13 Issue Supplement Pages 7-10

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Abstract
Isotope dilution-inductively coupled plasma mass spectrometry (ID-ICP-MS) was applied to the determination of lead in natural water, and its precision was compared to that of the conventional calibration method. Trace amount of lead in natural water was preconcentrated using a chelating resin of Chelex 100 before ID-ICP-MS, where the preconcentration factor of 50 was obtained. The concentrations of lead were 26.1pg/g and 266pg/g for the certified river reference materials (JAC 0031) and the pond water sample, respectively, with the RSD less than 1%.
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© The Japan Society for Analytical Chemistry
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