Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 6
Crystal Structure of [SiH2Mes2] (Mes = 2,4,6-trimethylphenyl)
Mohammad K. ROFOUEIGerard A. LAWLESSAli MORSALIPeter B. HITCHCOCK
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JOURNAL FREE ACCESS

2005 Volume 21 Pages x103-x104

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Abstract

The crystal structure properties of [SiH2Mes2] (Mes = 2,4,6-trimethylphenyl) are: monoclinic, space group C2/c with a = 13.221(6), b = 9.076(2), c = 13.448(5)Å, Z = 4, R1 = 0.054 and wR2 = 0.129 with 1727 reflections (I > 2σ(I)). The coordination geometry about Si is approximately tetrahedral with a C-Si-C angle of 114.14(11)°. There is π-π stacking interaction between the parallel aromatic rings.

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© 2005 by The Japan Society for Analytical Chemistry
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