Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 9
Crystal Structure of 4,4′-Dichloro-2,2′-[(1,4-butylene)dioxybis-(nitrilomethylidyne)]diphenol
Wei-Kui DONGJun-Yan SHIYin-Xia SUNLi WANGJin-Gui DUANJin-Kui ZHONGLi XU
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ジャーナル フリー

2007 年 23 巻 p. x167-x168

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抄録
The title compound, 4,4′-dichloro-2,2′-[(1,4-butylene)dioxybis(nitrilomethylidyne)]diphenol, was synthesized and characterized by single-crystal X-ray diffraction. It crystalizes in the monoclinic system, space group P21/n with a = 4.9390(7)Å, b = 30.235(3)Å, c = 6.1349(14)Å, β = 90.818(2)°, Z = 2, V = 916.0(3)Å3; the final residual factor is R = 0.0458 for 1613 measured reflections. The intramolecular O-H…N hydrogen bonds are dominantly effective in stabilizing the crystal structure.
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© 2007 by The Japan Society for Analytical Chemistry
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