Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 4
Synthesis and Structure of 3,3′-[(4-Bromophenyl)methylene]bis-[4-hydroxy-2H-1-benzopyran-2-one]
Ilia MANOLOVCäcilia MAICHLE-MÖSSMER
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2007 Volume 23 Pages x63-x64

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Abstract

The title compound, 3,3′-[(4-bromophenyl)methylene]bis-[4-hydroxy-2H-1-benzopyran-2-one], molecular formula C25H15BrO6, Mr = 491.28, crystallizes in the monoclinic system, space group P21/c, with cell constants a = 10.256(2)Å, b = 10.2341(17)Å, c = 19.839(5)Å, β = 93.61(2)°, V = 2078.1(8)Å3 and Z = 4, R1 = 0.0588. The 4-hydroxycoumarins are intramolecularly hydrogen bonded between hydroxyls and carbonyls.

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© 2007 by The Japan Society for Analytical Chemistry
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