バイオインテグレーション学会誌
Online ISSN : 2186-2923
Nitriding of a titanium surface by microwave plasma and formation of apatite in SBF
Jincheng BaiTakuma NagashimaTatsuhiko Yajima
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ジャーナル オープンアクセス

2016 年 5 巻 1 号 p. 73-78

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Carbon felt is composed of carbon fibers and, when calcined at high temperatures in the vicinity of 2000 °C or above, exhibits specific properties, including a large specific area, low electrical resistance and high microwave absorptivity. Recently, it was found that irradiation of a pair of disc-like carbon felts arranged in parallel with a ceramic ring spacer by 2.45 GHz microwaves (MW) under atmosphere air generates a thermal discharge plasma, termed a carbon felt atmospheric pressure microwave plasma (CAMP), at the gap between the felts. The temperature of the gap increases rapidly to reach thermal equilibrium at 1200 °C or higher in approximately 20 seconds, although the temperature at the circumference of felts can be as low as 200 °C 1). In the present study, the surface nitriding and oxynitridation of titanium by CAMP under atmospheric pressure nitrogen were successfully performed using carbon felts as a MW absorbing material. In addition, the formation of hydroxyapatite (HAp) by surface contact with a simulated body fluid (SBF) was assessed. The resulting surfaces of the titanium substrates were analyzed by X-ray photoelectron spectroscopy, X-ray diffraction and scanning electron microscopy.
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© 2016 Bio Integration Society
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