Separator-less One-compartment Bulk Electrolysis with a Small Auxiliary Electrode and its Application to Spectroelectrochemistry

Abstract

Separator-less one-compartment bulk electrolytic method, in which the area of the auxiliary electrode is sufficiently small compared with that of the working electrode, has been proposed. The method was also applied to spectroelectrochemical measurements. All electrochemical and spectrophotometric data have revealed that the method allows almost ideal and complete electrolysis.