抵抗炉法による高温単結晶X線回折実験について
1983 年 16 巻 Special 号 p. 5-11
詳細
1983 年 16 巻 Special 号 p. 5-11
The previously reported resistance heaters for the high-temperature single crystal X-ray diffraction study can be classified into two groups based on the characteristics of heater element employed. The elements which are able to use in the open air constitute one group. Platinum or nicrome wire resistance heaters belong to this group and these heaters are suitable for relatively low temperature experiments below 1100°C. Graphite heater and Tantalum heater constitute the other group and these heater elements are stable only under the vacuum or in the inert gas atmosphere. The elements in this group can generate temperatures higher than 2000°C. Two selected designs of heaters were described from each group. A high-temperature cement and a method for mounting sample crystal are also described.
