1963 年 5 巻 4 号 p. 272-279
An approach to recover UO2 mechanically from the UO2-graphite fuel specimen was investigated. After disintegrating an unirradiated specimen by a pulverizer, ball mill, or micron mill, the obtained powder was separated into the UO2 and graphite phases by a heavy-media-separation method in which a zinc-bromide solution was used as the heavy medium.
The disintegration of the specimen into fine powder was essential for the mechanical separation of UO2.
Additional treatments such as preoxidation of the sample, addition of dispersion agent to the zinc-bromide solution, and irradiation of the solution with the ultrasonic waves, were not effective in improving the UO2 recovery.
However, it seemed that the grinding method coupled with continuous removal of the ground particles with fluid flowing would be effective in obtaining a high UO2 recovery.