石炭科学会議発表論文集
Online ISSN : 2423-8309
Print ISSN : 2423-8295
ISSN-L : 2423-8295
第40回石炭科学会議
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28.マイクロ波照射酸分解法による石炭中の微量金属の定量分析
王 杰坂西 欣也中里 哲也田尾 博明山田 理斎藤 郁夫
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p. 58-59

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The purpose of study is to develop standard methods for analysis of trace elements in coal by ICP-OES and ICP-MS combined with microwave-assisted digestion. It is strongly needed to develop safe and efficient digestion methods compatible with the instrumental analyses. In this study, we try to use a mixture of HNO_3 and H_2O_2 as coal digestion reagents. The use of this simple mixture without addition of conventionally used reagents HF, HCl or HClO_4 is favorable to a stable and simple instrumental operation. It was interesting to find that almost all the trace elements examined were successfully determined with reference to three standard coals.

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